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Light-driven high-temperature continuous-flow synthesis of TiO2 nano-anatase
journal contribution
posted on 2023-05-17, 15:48 authored by Chan, BCY, Xiaolin WangXiaolin Wang, Lam, LKW, Gordan, JM, Feuermann, D, Raston, CL, Chua, HTDeveloping continuous-flow high-temperature fabrication strategies constitutes a pivotal challenge in the realization and scale-up of some functional nanomaterials. We have developed a light-driven large-area spinning-disk processor for this purpose, and establish its continuous-flow capability in preparing TiO2 anatase-phase nanoparticles with reaction temperatures up to 550°C. This reactor strategy markedly reduces reaction time – primarily by eliminating the need for product calcination – while maintaining high conversion efficiency. A fundamentally new reactor strategy for nanomaterial synthesis is reported. The key is conflating unorthodox optics with spinning disk processors. Experimental results and structural characterization are for TiO2 nano-anatase. We depict a continuous-flow high-temperature strategy for nanomaterial generation.
History
Publication title
Chemical Engineering JournalVolume
211-212Pagination
195-199ISSN
1385-8947Department/School
School of EngineeringPublisher
ElsevierPlace of publication
InternationalRights statement
Copyright 2012 Elsevier B.V.Repository Status
- Restricted