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Solid-phase micro-extraction - comprehensive two-dimensional gas chromatography of ginger (Zingiber Officinale) volatiles

Citation

Shao, Y and Marriott, P and Shellie, RA and Hugel, H, Solid-phase micro-extraction - comprehensive two-dimensional gas chromatography of ginger (Zingiber Officinale) volatiles, Flavour and Fragrance Journal, 18, (1) pp. 5-12. ISSN 0882-5734 (2003) [Refereed Article]


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The definitive published version is available online at: http://interscience.wiley.com

DOI: doi:10.1002/ffj.1133

Abstract

Ginger (Zingiber officinale) headspace has been studied by using solid-phase microextraction (SPME), combined with comprehensive two-dimensional (2D) gas chromatography (GC GC). A 100 m PDMS fibre proved to be the most useful in the present study. SPME-GC-MS analysis was also performed to identify the components extracted from the volatile fraction. The ease of SPME makes it a useful tool for qualitative comparison of samples, and here fresh ginger was contrasted with a crystallized ginger sweet. The latter sample had fewer of the more volatile components, but the heavier components appeared to compare well in the two samples. The use of SPME as a sample introduction method for GC GC was investigated, using the two different ginger samples. The correspondence of retention times in the 2D separation space was found to be excellent, and should allow reliable identification of the compounds if adequate standards or comparative retentions of known components are available.

Item Details

Item Type:Refereed Article
Keywords:GC GC multidimensional GC GC-MS ginger essential oil cryogenic modulation
Research Division:Chemical Sciences
Research Group:Analytical Chemistry
Research Field:Separation Science
Objective Division:Manufacturing
Objective Group:Instrumentation
Objective Field:Scientific Instruments
Author:Shellie, RA (Associate Professor Robert Shellie)
ID Code:36245
Year Published:2003
Web of Science® Times Cited:38
Deposited By:Chemistry
Deposited On:2005-11-15
Last Modified:2010-03-16
Downloads:9 View Download Statistics

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