A parts-per-million level screening technique for bis(chloromethyl)ether using micromachined differential ion mobility spectrometry combined with portable temperature programmable low thermal mass silicon micromachined gas chromatography is described. With its capability to operate in atmospheric pressure, the analytical system affords fast start-up with a high sample throughput. The technique described can be used to screen for bis(chloromethyl)ether in ambient air directly without pre-concentration or derivatization with a low possibility of false positive results. A complete analysis can be carried out in less than 240 s. A detection limit of 2 μL L⁻¹ and relative precision of less than 5% RSD (n = 10) over a range from 5 μL L⁻¹ to 500 μL L⁻¹ were obtained.

Item Type:	Refereed Article
Keywords:	spectrometry, gas chromatography, bis(chloromethyl)ether detection
Research Division:	Chemical Sciences
Research Group:	Analytical Chemistry
Research Field:	Separation Science
Objective Division:	Manufacturing
Objective Group:	Instrumentation
Objective Field:	Scientific Instruments
Author:	Luong, J (Mr Jim Luong)
Author:	Gras, R (Ms Ronda Gras)
Author:	Shellie, RA (Associate Professor Robert Shellie)
ID Code:	123659
Year Published:	2017
Deposited By:	Austn Centre for Research in Separation Science
Deposited On:	2018-01-17
Last Modified:	2018-03-28
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